FOOD ANALYSIS Content Preface and Acknowledgments Notes on Calculations of Concentration 1 Nutrition Labeling Using a Computer Program A Preparing Nutrition Labels for SampleYogurt Formulas B Adding New Ingredients to a Formula and Determining How They Influence the Nutrition Label C An Example of Reverse Engineering in Product Development 2 Assessment of Accuracy and Precision 3 Determination of Moisture Content A Forced Draft Oven B Vacuum Oven C Microwave Drying Oven D Rapid Moisture Analyzer E Toluene Distillation F Karl Fischer G Near Infrared Analyzer 4 Determination of Fat Content A Soxhlet Method B Goldfish Method C Mojonnier Method D Babcock Method 5 Protein Nitrogen Determination A Kjeldahl Nitrogen Method B Nitrogen Combustion Method 6 Phenol-Sulfuric Acid Method forTotal Carbohydrates 7 Vitamin C Determination by Indophenol Method 8 Complexometric Determination of Calcium A EDTA Titrimetric Method for Testing Hardness of Water B Test Strips for Water Hardness 9 Iron Determination in Meat Using Ferrozine Assay 10 Sodium Determination Using Ion Selective Electrodes, Mohr Titration, and Test Strips A Ion Selective Electrodes B Mohr Titration C Quantab® Test Strips 11 Sodium and Potassium Determinations by AtomicAbsorption Spectroscopy and Inductively Coupled Plasma-Atomic Emission Spectroscopy 12 Standard Solutions and Titratable Acidity A Preparation and Standardization of Base and Acid Solutions B Titratable Acidity and pH 13 Fat Characterization A Saponification Value B Iodine Value C Free Fatty Acid Value D Peroxide Value E Thin-Layer Chromatography Separation of Simple Lipids 14 Fish Muscle Proteins: Extraction, Quantitation, and Electrophoresis 15 Enzyme Analysis to Determine Glucose 16 Gliadin Detection in Food by Immunoassay 17 Examination of Foods for Extraneous Materials A Extraneous Matter in Soft Cheese B Extraneous Matter in Jam 140 C Extraneous Matter in Infant Food D Extraneous Matter in Potato Chips E Extraneous Matter in Citrus Juice 18 High Performance Liquid Chromatography A Determination of Caffeine in Beverages by HPLC B Solid-Phase Extraction and HPLC Analysis of Anthocyanidins from Fruits and Vegetables 19 Gas Chromatography A Determination of Methanol and Higher Alcohols In Wine by Gas Chromatography B Preparation of Fatty Acid Methyl Esters (FAMEs), and Determination of Fatty Acid Profile of Oils by Gas Chromatography 20 Viscosity Measurement Using a Brookfield Viscometer 21 Calculation of CIE Color Specifications from Reflectance or Transmittance Spectra
FOOD ANALYSIS
Content
Preface and Acknowledgments
Notes on Calculations of Concentration
1 Nutrition Labeling Using a Computer Program
A Preparing Nutrition Labels for SampleYogurt Formulas
B Adding New Ingredients to a Formula and Determining How They Influence the Nutrition Label
C An Example of Reverse Engineering in Product Development
2 Assessment of Accuracy and Precision
3 Determination of Moisture Content
A Forced Draft Oven
B Vacuum Oven
C Microwave Drying Oven
D Rapid Moisture Analyzer
E Toluene Distillation
F Karl Fischer
G Near Infrared Analyzer
4 Determination of Fat Content
A Soxhlet Method
B Goldfish Method
C Mojonnier Method
D Babcock Method
5 Protein Nitrogen Determination
A Kjeldahl Nitrogen Method
B Nitrogen Combustion Method
6 Phenol-Sulfuric Acid Method forTotal Carbohydrates
7 Vitamin C Determination by Indophenol Method
8 Complexometric Determination of Calcium
A EDTA Titrimetric Method for Testing Hardness of Water
B Test Strips for Water Hardness
9 Iron Determination in Meat Using Ferrozine Assay
10 Sodium Determination Using Ion Selective Electrodes, Mohr Titration, and Test Strips
A Ion Selective Electrodes
B Mohr Titration
C Quantab® Test Strips
11 Sodium and Potassium Determinations by AtomicAbsorption Spectroscopy and Inductively Coupled Plasma-Atomic Emission Spectroscopy
12 Standard Solutions and Titratable Acidity
A Preparation and Standardization of Base and Acid Solutions
B Titratable Acidity and pH
13 Fat Characterization
A Saponification Value
B Iodine Value
C Free Fatty Acid Value
D Peroxide Value
E Thin-Layer Chromatography Separation of Simple Lipids
14 Fish Muscle Proteins: Extraction, Quantitation, and Electrophoresis
15 Enzyme Analysis to Determine Glucose
16 Gliadin Detection in Food by Immunoassay
17 Examination of Foods for Extraneous Materials
A Extraneous Matter in Soft Cheese
B Extraneous Matter in Jam 140
C Extraneous Matter in Infant Food
D Extraneous Matter in Potato Chips
E Extraneous Matter in Citrus Juice
18 High Performance Liquid Chromatography
A Determination of Caffeine in Beverages by HPLC
B Solid-Phase Extraction and HPLC Analysis of Anthocyanidins from Fruits and Vegetables
19 Gas Chromatography
A Determination of Methanol and Higher Alcohols In Wine by Gas Chromatography
B Preparation of Fatty Acid Methyl Esters (FAMEs), and Determination of Fatty Acid Profile of Oils by Gas Chromatography
20 Viscosity Measurement Using a Brookfield Viscometer
21 Calculation of CIE Color Specifications from Reflectance or Transmittance Spectra
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